Information card for entry 7104503

Structure parameters

• Formula: C26 H48 Li N O2 Si Zn
• Calculated formula: C26 H48 Li N O2 Si Zn
• Title of publication: Direct lateral metallation using alkali-metal mediated zincation (AMMZn): SiC-H vs.Si-O bond cleavage.
• Authors of publication: Hevia, Eva; Kennedy, Alan R; Klett, Jan; McCall, Matthew D
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 22
• Pages of publication: 3240 - 3242
• a: 11.2813 ± 0.0005 Å
• b: 11.37 ± 0.0006 Å
• c: 13.0987 ± 0.0006 Å
• α: 79.264 ± 0.004°
• β: 79.106 ± 0.004°
• γ: 61.575 ± 0.005°
• Cell volume: 1441.91 ± 0.12 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0472
• Residual factor for significantly intense reflections: 0.0314
• Weighted residual factors for significantly intense reflections: 0.0695
• Weighted residual factors for all reflections included in the refinement: 0.0725
• Goodness-of-fit parameter for all reflections included in the refinement: 0.967
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No