Information card for entry 7104660

Structure parameters

• Formula: C28 H31 O4 Rh
• Calculated formula: C28 H31 O4 Rh
• Title of publication: Electronic and steric tuning of chiral diene ligands for rhodium-catalyzed asymmetric arylation of imines.
• Authors of publication: Okamoto, Kazuhiro; Hayashi, Tamio; Rawal, Viresh H
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 32
• Pages of publication: 4815 - 4817
• a: 6.7928 ± 0.0007 Å
• b: 8.4033 ± 0.0008 Å
• c: 41.694 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2380 ± 0.4 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 4
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0453
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.0939
• Weighted residual factors for all reflections included in the refinement: 0.0944
• Goodness-of-fit parameter for all reflections included in the refinement: 1.319
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No