Information card for entry 7104667

Structure parameters

• Formula: C137 H100 Cr F28.5 N33.5 O1.2 P5 V4
• Calculated formula: C137 H100 Cr F28.5 N33.5 O1.24 P5 V4
• Title of publication: Strong magnetic exchange coupling in the cyano-bridged coordination clusters [(PY5Me2)4V4M(CN)6]5+ (M = Cr, Mo).
• Authors of publication: Freedman, Danna E; Jenkins, David M; Long, Jeffrey R
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 32
• Pages of publication: 4829 - 4831
• a: 33.307 ± 0.001 Å
• b: 33.307 ± 0.001 Å
• c: 28.8894 ± 0.0017 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 32049 ± 2 ų
• Cell temperature: 156 K
• Ambient diffraction temperature: 156 K
• Number of distinct elements: 8
• Space group number: 140
• Hermann-Mauguin space group symbol: I 4/m c m
• Hall space group symbol: -I 4 2c
• Residual factor for all reflections: 0.1237
• Residual factor for significantly intense reflections: 0.0989
• Weighted residual factors for significantly intense reflections: 0.2882
• Weighted residual factors for all reflections included in the refinement: 0.3159
• Goodness-of-fit parameter for all reflections included in the refinement: 2.675
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No