Information card for entry 7104674

Structure parameters

• Formula: C78 H81 Ge2 O5.5
• Calculated formula: C78 H81 Ge2 O5.5
• Title of publication: An isolable o-quinodimethane and its fixation of molecular oxygen to give an endoperoxide.
• Authors of publication: Ghereg, Dumitru; Ech-Cherif El Kettani, Sakina; Lazraq, Mohamed; Ranaivonjatovo, Henri; Schoeller, Wolfgang W; Escudié, Jean; Gornitzka, Heinz
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal volume: 34
• Journal issue: 32
• Pages of publication: 4821 - 4823
• a: 9.8547 ± 0.0006 Å
• b: 14.9574 ± 0.0009 Å
• c: 23.1368 ± 0.0015 Å
• α: 71.149 ± 0.001°
• β: 83.026 ± 0.001°
• γ: 81.414 ± 0.001°
• Cell volume: 3181.5 ± 0.3 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1366
• Residual factor for significantly intense reflections: 0.0612
• Weighted residual factors for significantly intense reflections: 0.1117
• Weighted residual factors for all reflections included in the refinement: 0.1376
• Goodness-of-fit parameter for all reflections included in the refinement: 0.978
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No