Information card for entry 7104805

Structure parameters

• Formula: C76 H66 B Cl2 F24 N3 Pd
• Calculated formula: C76 H66 B Cl2 F24 N3 Pd
• Title of publication: The first Pd^II^ complex of a non-heteroatom stabilised carbene ligand
• Authors of publication: Bröring, Martin; Brandt, Carsten D.; Stellwag, Sascha
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2003
• Journal issue: 18
• Pages of publication: 2344 - 2345
• a: 14.643 ± 0.0004 Å
• b: 15.2381 ± 0.0005 Å
• c: 18.371 ± 0.0005 Å
• α: 88.151 ± 0.002°
• β: 73.782 ± 0.002°
• γ: 78.955 ± 0.002°
• Cell volume: 3862.1 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1194
• Residual factor for significantly intense reflections: 0.1063
• Weighted residual factors for significantly intense reflections: 0.2075
• Weighted residual factors for all reflections included in the refinement: 0.211
• Goodness-of-fit parameter for all reflections included in the refinement: 1.441
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No