Information card for entry 7105044

Structure parameters

• Common name: (DIPP-nacnac)MgNH(DIPP)BH3
• Formula: C41 H62 B Mg N3
• Calculated formula: C41 H62 B Mg N3
• Title of publication: Synthesis and structure of a magnesium-amidoborane complex and its role in catalytic formation of a new bis-aminoborane ligand.
• Authors of publication: Spielmann, Jan; Bolte, Michael; Harder, Sjoerd
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2009
• Journal issue: 45
• Pages of publication: 6934 - 6936
• a: 18.295 ± 0.004 Å
• b: 11.8119 ± 0.0014 Å
• c: 18.846 ± 0.003 Å
• α: 90°
• β: 103.004 ± 0.015°
• γ: 90°
• Cell volume: 3968.2 ± 1.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2345
• Residual factor for significantly intense reflections: 0.0924
• Weighted residual factors for significantly intense reflections: 0.1824
• Weighted residual factors for all reflections included in the refinement: 0.2375
• Goodness-of-fit parameter for all reflections included in the refinement: 0.874
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No