Information card for entry 7105111

Structure parameters

• Formula: H172 K18 Mo12 Na14 O298 P8 W48
• Calculated formula: K16 Mo12 Na12 O275.16 P8 W48
• Title of publication: Vectorial growth/regulations in a {P8W48}-type polyoxotungstate compartment: trapped unusual molybdenum oxide acts as a handle
• Authors of publication: Filipa L. Sousa; Hartmut Bögge; Alice Merca; Pierre Gouzerh; René Thouvenot; Achim Müller
• Journal of publication: Chem. Commun.
• Year of publication: 2009
• Pages of publication: 7491 - 7493
• a: 25.6839 ± 0.0008 Å
• b: 25.6839 ± 0.0008 Å
• c: 22.0032 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 14514.7 ± 0.9 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 7
• Space group number: 87
• Hermann-Mauguin space group symbol: I 4/m
• Hall space group symbol: -I 4
• Residual factor for all reflections: 0.0575
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for significantly intense reflections: 0.1299
• Weighted residual factors for all reflections included in the refinement: 0.1451
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No