Information card for entry 7105323

Structure parameters

• Formula: C54 H122 Pb4 Sb6 Si6
• Calculated formula: C54 H122 Pb4 Sb6 Si6
• Title of publication: Synthesis of molecular lead-pnictogen compounds including [Pb4(SbSiiPr3)6], the first structurally characterised compound with a lead-antimony bond.
• Authors of publication: Traut, Stephan; von Hänisch, Carsten
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 9
• Pages of publication: 1538 - 1540
• a: 23.786 ± 0.005 Å
• b: 13.266 ± 0.003 Å
• c: 26.391 ± 0.005 Å
• α: 90°
• β: 105.03 ± 0.03°
• γ: 90°
• Cell volume: 8043 ± 3 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0565
• Residual factor for significantly intense reflections: 0.0458
• Weighted residual factors for significantly intense reflections: 0.1134
• Weighted residual factors for all reflections included in the refinement: 0.1181
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No