Information card for entry 7105551

Structure parameters

• Formula: C43.5 H110 Co N6 O47.5
• Calculated formula: C43.5 Co N6 O47.5
• Title of publication: Crystal structure and chiral recognition of supramolecular complex composed of tris(1,2-diaminoethane)cobalt(iii) carbonate and α-cyclodextrin, [Co(en)3]2(CO3)3·2(α-CDX)
• Authors of publication: Ohta, Natsuki; Fuyuhiro, Akira; Yamanari, Kazuaki
• Journal of publication: Chemical Communications
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 20
• Pages of publication: 3535
• a: 13.8755 ± 0.0003 Å
• b: 17.7282 ± 0.0003 Å
• c: 17.4932 ± 0.0003 Å
• α: 77.41 ± 0.013°
• β: 66.587 ± 0.014°
• γ: 65.518 ± 0.013°
• Cell volume: 3586.5 ± 0.5 ų
• Cell temperature: 200 K
• Number of distinct elements: 5
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for significantly intense reflections: 0.1368
• Weighted residual factors for all reflections included in the refinement: 0.3981
• Goodness-of-fit parameter for all reflections included in the refinement: 1.467
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoK06a
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No