Information card for entry 7105586

Structure parameters

• Formula: C38 H61 B2 Li N2 O5 Si
• Calculated formula: C38 H61 B2 Li N2 O5 Si
• Title of publication: Lewis-base adducts of 9,10-dihydro-9,10-diboraanthracene: ditopic hydroboration reagents and a B-N analogue of triptycene.
• Authors of publication: Lorbach, Andreas; Bolte, Michael; Lerner, Hans-Wolfram; Wagner, Matthias
• Journal of publication: Chemical communications (Cambridge, England)
• Year of publication: 2010
• Journal volume: 46
• Journal issue: 20
• Pages of publication: 3592 - 3594
• a: 10.0824 ± 0.0012 Å
• b: 17.4274 ± 0.0015 Å
• c: 12.4327 ± 0.0016 Å
• α: 90°
• β: 110.322 ± 0.009°
• γ: 90°
• Cell volume: 2048.6 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0856
• Residual factor for significantly intense reflections: 0.0666
• Weighted residual factors for significantly intense reflections: 0.1706
• Weighted residual factors for all reflections included in the refinement: 0.1822
• Goodness-of-fit parameter for all reflections included in the refinement: 0.956
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No