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Information card for entry 7105653
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Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 7105653.cif |
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Original paper (by DOI) | HTML |
Formula | C19 H22 B I O2 S |
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Calculated formula | C19 H22 B I O2 S |
Title of publication | Selective synthesis of dibenzo[a,c]cyclooctatetraenes via palladium-catalyzed [4+4] cyclic homocoupling of borylvinyl iodobenzene derivatives. |
Authors of publication | Zhang, Hui-jun; Wei, Junnian; Zhao, Fei; Liang, Yun; Wang, Zitao; Xi, Zhenfeng |
Journal of publication | Chemical communications (Cambridge, England) |
Year of publication | 2010 |
Journal volume | 46 |
Journal issue | 39 |
Pages of publication | 7439 - 7441 |
a | 7.7475 ± 0.0004 Å |
b | 14.4249 ± 0.0008 Å |
c | 34.686 ± 0.002 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 3876.4 ± 0.4 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 6 |
Space group number | 61 |
Hermann-Mauguin space group symbol | P b c a |
Hall space group symbol | -P 2ac 2ab |
Residual factor for all reflections | 0.0536 |
Residual factor for significantly intense reflections | 0.047 |
Weighted residual factors for significantly intense reflections | 0.0988 |
Weighted residual factors for all reflections included in the refinement | 0.1024 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.151 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7105653.html
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