Information card for entry 7105675

Structure parameters

• Formula: C20 H36 P2 Pd
• Calculated formula: C20 H36 P2 Pd
• Title of publication: Selective Reduction of a Pd Pincer PCP Complex to Well-Defined Pd(0) Species
• Authors of publication: Crisobal Melero; Luis Martinez-Prieto; Pilar Palma; Diego del Rio; Eleuterio Alvarez; Juan Campora
• Journal of publication: Chem.Commun.
• Year of publication: 2010
• Journal volume: 46
• Pages of publication: 8851
• a: 12.984 ± 0.004 Å
• b: 11.268 ± 0.003 Å
• c: 15.661 ± 0.005 Å
• α: 90°
• β: 99.864 ± 0.008°
• γ: 90°
• Cell volume: 2257.4 ± 1.2 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0983
• Residual factor for significantly intense reflections: 0.0639
• Weighted residual factors for significantly intense reflections: 0.1618
• Weighted residual factors for all reflections included in the refinement: 0.2374
• Goodness-of-fit parameter for all reflections included in the refinement: 1.09
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No