Information card for entry 7105711

Structure parameters

• Formula: C155 H112 Au8 Cl6 F12 O2 P10
• Calculated formula: C155 H112 Au8 Cl6 F12 O2 P10
• Title of publication: Assembly of the Au–diphosphine helical cage molecules via alkynyl–?4-methylydine ligand transformation (C152 H142 Au8 F12 N2 O5 P10 and C155 H112 Au8 Cl6 F12 O2 P10)
• Authors of publication: Igor Koshevoy; Matti Haukka; Stanislav Selivanov; Sergey Tunik; Tapani Pakkanen
• Journal of publication: Chem.Commun.
• Year of publication: 2010
• Journal volume: 46
• Pages of publication: 8926
• a: 20.8064 ± 0.0004 Å
• b: 20.5555 ± 0.0005 Å
• c: 36.4529 ± 0.0009 Å
• α: 90°
• β: 91.848 ± 0.001°
• γ: 90°
• Cell volume: 15582.3 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0663
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.0884
• Weighted residual factors for all reflections included in the refinement: 0.0955
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No