Information card for entry 7106058

Structure parameters

• Formula: C32 H29 F12 Fe N11 P2
• Calculated formula: C30 H26 F12 Fe N10 P2
• Title of publication: Facile Synthesis of Metal N-Heterocyclic Carbene Complexes
• Authors of publication: Bin Liu; Yin Zhang; Daichao Xu; Wanzhi Chen
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 2883
• a: 9.67 ± 0.0019 Å
• b: 12.62 ± 0.003 Å
• c: 17.4 ± 0.004 Å
• α: 99.94 ± 0.03°
• β: 100.94 ± 0.03°
• γ: 110.39 ± 0.03°
• Cell volume: 1887.3 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1615
• Residual factor for significantly intense reflections: 0.1144
• Weighted residual factors for significantly intense reflections: 0.3355
• Weighted residual factors for all reflections included in the refinement: 0.3609
• Goodness-of-fit parameter for all reflections included in the refinement: 1.159
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No