Information card for entry 7106146

Structure parameters

• Formula: C69.5 H55 B2 F26.5 N P2 Rh
• Calculated formula: C69.5 H55 B2 F26.5 N P2 Rh
• Title of publication: Tuning the [L2RhH3B·NR3]+ interaction using phosphine bite angle. Demonstration by the catalytic formation of polyaminoboranes
• Authors of publication: Romaeo Dallanegra Alasdair P. M. Robertson Adrian B. Chaplin Ian Manners Andrew S. Weller
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 3763
• a: 12.9731 ± 0.0002 Å
• b: 17.4492 ± 0.0002 Å
• c: 18.3033 ± 0.0003 Å
• α: 110.137 ± 0.0006°
• β: 95.378 ± 0.0007°
• γ: 99.4374 ± 0.0007°
• Cell volume: 3786.61 ± 0.1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0629
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for significantly intense reflections: 0.1455
• Weighted residual factors for all reflections included in the refinement: 0.1541
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No