Information card for entry 7106159

Structure parameters

• Formula: C22 H32 I O10.5
• Calculated formula: C22 H32 I O10.5
• Title of publication: Enantioselective Prevost and Woodward reactions using chiral hypervalent iodine(III): switchover of stereochemical course of an optically active 1,3-dioxolan-2-yl cation
• Authors of publication: Morifumi Fujita; Mikimasa Wakita; Takashi Sugimura
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 3983
• a: 23.3688 ± 0.0011 Å
• b: 23.3688 ± 0.0011 Å
• c: 8.5888 ± 0.0002 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4062 ± 0.3 ų
• Cell temperature: 293.1 K
• Ambient diffraction temperature: 293.1 K
• Number of distinct elements: 4
• Space group number: 170
• Hermann-Mauguin space group symbol: P 65
• Hall space group symbol: P 65
• Residual factor for significantly intense reflections: 0.0517
• Weighted residual factors for all reflections included in the refinement: 0.0577
• Goodness-of-fit parameter for all reflections included in the refinement: 1.188
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No