Information card for entry 7106324

Structure parameters

• Chemical name: Octakis[3-{pyrid-2-yl}-5-tertbutylpyrazolyl]decasilver(I) dichloride
• Formula: C96 H112 Ag10 Cl2 N24
• Calculated formula: C96 H112 Ag10 Cl1.4 N24
• Title of publication: New Insights into the Aggregation of Silver Pyrazolides Using Sterically Hindered Bidentate Pyrazole Ligands
• Authors of publication: James J. Henkelis; Colin A. Kilner; Malcolm A. Halcrow
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 5187
• a: 25.17 ± 0.002 Å
• b: 17.888 ± 0.0014 Å
• c: 24.0804 ± 0.0018 Å
• α: 90°
• β: 100.925 ± 0.004°
• γ: 90°
• Cell volume: 10645.5 ± 1.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1106
• Residual factor for significantly intense reflections: 0.0838
• Weighted residual factors for significantly intense reflections: 0.2603
• Weighted residual factors for all reflections included in the refinement: 0.286
• Goodness-of-fit parameter for all reflections included in the refinement: 1.117
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No