Information card for entry 7106383

Structure parameters

• Formula: C29 H41 F N2 Pb
• Calculated formula: C29 H41 F N2 Pb
• Title of publication: Pentafluoropyridine as a fluorinating reagent for preparing a hydrocarbon soluble ?-diketiminatolead(II) monofluoride
• Authors of publication: Anukul Jana; Sankaranarayana Pillai Sarish; Herbert W. Roesky; Dirk Leusser; Ina Objartel; Dietmar Stalke
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 5434
• a: 11.7697 ± 0.0016 Å
• b: 20.465 ± 0.003 Å
• c: 11.7727 ± 0.0016 Å
• α: 90°
• β: 95.906 ± 0.002°
• γ: 90°
• Cell volume: 2820.6 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0256
• Residual factor for significantly intense reflections: 0.021
• Weighted residual factors for significantly intense reflections: 0.0491
• Weighted residual factors for all reflections included in the refinement: 0.0503
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No