Information card for entry 7106421

Structure parameters

• Formula: C30 H56 Li2 N10 Sn2
• Calculated formula: C30 H56 Li2 N10 Sn2
• Title of publication: Oxidative Dehydrocoupling of N-H Bonds Using a Redox-Active Main Group Superbase
• Authors of publication: R.J.Less; V.Naseri; M.McPartlin; D.S.Wright
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 6129
• a: 13.9707 ± 0.0003 Å
• b: 9.3155 ± 0.0002 Å
• c: 14.8029 ± 0.0003 Å
• α: 90°
• β: 106.888 ± 0.001°
• γ: 90°
• Cell volume: 1843.43 ± 0.07 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0559
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0794
• Weighted residual factors for all reflections included in the refinement: 0.0869
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No