Information card for entry 7106454

Structure parameters

• Formula: C55 H71 Cu F6 N P2 Sb
• Calculated formula: C55 H71 Cu F6 N P2 Sb
• Title of publication: Synthesis and coordination behavior of Cy(I) bis(phosphaethenyl)pyridine complexes.
• Authors of publication: Yumiko Nakajima; Yu Shiraishi; Takahiro Tsuchimoto; Fumiyuki Ozawa
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 6332
• a: 11.715 ± 0.002 Å
• b: 24.683 ± 0.005 Å
• c: 19.4 ± 0.004 Å
• α: 90°
• β: 106.209 ± 0.003°
• γ: 90°
• Cell volume: 5386.7 ± 1.8 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1036
• Residual factor for significantly intense reflections: 0.0875
• Weighted residual factors for significantly intense reflections: 0.227
• Weighted residual factors for all reflections included in the refinement: 0.2367
• Goodness-of-fit parameter for all reflections included in the refinement: 1.396
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No