Information card for entry 7106456

Structure parameters

• Formula: C57 H73 Cl2 Cu F6 N O P2 Sb
• Calculated formula: C57 H73 Cl1.98 Cu F6 N O P2 Sb
• Title of publication: Synthesis and coordination behavior of Cy(I) bis(phosphaethenyl)pyridine complexes.
• Authors of publication: Yumiko Nakajima; Yu Shiraishi; Takahiro Tsuchimoto; Fumiyuki Ozawa
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 6332
• a: 18.33 ± 0.007 Å
• b: 18.284 ± 0.006 Å
• c: 18.673 ± 0.007 Å
• α: 90°
• β: 110.23 ± 0.004°
• γ: 90°
• Cell volume: 5872 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.1099
• Residual factor for significantly intense reflections: 0.1005
• Weighted residual factors for significantly intense reflections: 0.3153
• Weighted residual factors for all reflections included in the refinement: 0.3193
• Goodness-of-fit parameter for all reflections included in the refinement: 1.992
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No