Information card for entry 7106727

Structure parameters

• Formula: C18 H52 I N3 Si6 U
• Calculated formula: C18 H52 I N3 Si6 U
• SMILES: [U]1(I)(N([Si](C)(C)C)[Si](C)(C)CC[Si](N1[Si](C)(C)C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: Towards high-valent uranium compounds from metallacyclic uranium(IV) precursors
• Authors of publication: Olivier Benaud; Jean-Claude Berthet; Pierre Thuery; Michel Ephritikhine
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 9057
• a: 11.8236 ± 0.0004 Å
• b: 14.8539 ± 0.0003 Å
• c: 19.3326 ± 0.0008 Å
• α: 90°
• β: 93.401 ± 0.002°
• γ: 90°
• Cell volume: 3389.34 ± 0.19 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0271
• Residual factor for significantly intense reflections: 0.0219
• Weighted residual factors for significantly intense reflections: 0.0539
• Weighted residual factors for all reflections included in the refinement: 0.0553
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No