Information card for entry 7106734

Structure parameters

• Formula: C120 H176 Fe4 N16 Si8 U4
• Calculated formula: C120 H176 Fe4 N16 Si8 U4
• Title of publication: Molecular quadrangle formation from a diuranium m-e⁶,e⁶-toluene complex
• Authors of publication: Marisa J. Monreal; Saeed I. Khan; Jaqueline L. Kiplinger; Paula L. Diaconescu
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 9119
• a: 35.332 ± 0.007 Å
• b: 35.332 ± 0.007 Å
• c: 38.836 ± 0.008 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 41986 ± 15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0911
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for significantly intense reflections: 0.1442
• Weighted residual factors for all reflections included in the refinement: 0.158
• Goodness-of-fit parameter for all reflections included in the refinement: 0.946
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No