Information card for entry 7106800

Structure parameters

• Formula: C88 H92 Cu4 F24 N16 O P4
• Calculated formula: C88 H92 Cu4 F24 N16 O P4
• Title of publication: Synthesis and optical resolution of a Cu(I) double-stranded helicate with ketimine-bridged tris(bipyridine) ligands
• Authors of publication: Yoshio Furusho; Hidetoshi Goto; Ken Itomi; Hiroshi Katagiri; Toyoharu Miyagawa; Eiji Yashima
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 9795
• a: 32.027 ± 0.009 Å
• b: 11.894 ± 0.003 Å
• c: 24.907 ± 0.007 Å
• α: 90°
• β: 107.539 ± 0.003°
• γ: 90°
• Cell volume: 9047 ± 4 ų
• Cell temperature: 90 K
• Ambient diffraction temperature: 90 K
• Number of distinct elements: 7
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/c 1
• Hall space group symbol: -P 2yc
• Residual factor for all reflections: 0.1791
• Residual factor for significantly intense reflections: 0.1338
• Weighted residual factors for significantly intense reflections: 0.2857
• Weighted residual factors for all reflections included in the refinement: 0.3032
• Goodness-of-fit parameter for all reflections included in the refinement: 1.168
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No