Information card for entry 7106848

Structure parameters

• Common name: (RO)3VNNV(OR)3
• Formula: C30 H63 N O3 V
• Calculated formula: C30 H63 N O3 V
• Title of publication: Dinitrogen binding at vanadium in a tris(alkoxide) ligand environment
• Authors of publication: Stanislav Groysman; Dino Villagran; Danna Freedman; Daniel G. Nocera
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 10242
• a: 12.159 ± 0.0008 Å
• b: 15.1818 ± 0.0009 Å
• c: 17.6527 ± 0.0011 Å
• α: 82.418 ± 0.001°
• β: 82.061 ± 0.001°
• γ: 79.796 ± 0.001°
• Cell volume: 3157 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0823
• Residual factor for significantly intense reflections: 0.0521
• Weighted residual factors for significantly intense reflections: 0.1206
• Weighted residual factors for all reflections included in the refinement: 0.1384
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No