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Information card for entry 7106885
Preview
Coordinates | 7106885.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C20 H38 B Cl F4 N2 Ni P2 |
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Calculated formula | C20 H38 B Cl F4 N2 Ni P2 |
SMILES | [Ni](Cl)([P](CC)(CC)CC)([P](CC)(CC)CC)=C1N(c2c(N1)cccc2)C.[B](F)(F)(F)[F-] |
Title of publication | Synthesis of complexes bearing NH,NMe-substituted NHCs by oxidative addition of 2-halogenato-N-methylbenzimidazoles to Ni0+ |
Authors of publication | Tim Kosterke; Tania Pape; F. Ekkehardt Hahn |
Journal of publication | Chem.Commun. |
Year of publication | 2011 |
Journal volume | 47 |
Pages of publication | 10773 |
a | 9.1013 ± 0.0005 Å |
b | 30.6853 ± 0.0018 Å |
c | 9.4384 ± 0.0006 Å |
α | 90° |
β | 90.129 ± 0.001° |
γ | 90° |
Cell volume | 2635.9 ± 0.3 Å3 |
Cell temperature | 153 ± 2 K |
Ambient diffraction temperature | 153 ± 2 K |
Number of distinct elements | 8 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0558 |
Residual factor for significantly intense reflections | 0.0389 |
Weighted residual factors for significantly intense reflections | 0.0997 |
Weighted residual factors for all reflections included in the refinement | 0.1032 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.953 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/7106885.html
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