Information card for entry 7107059

Structure parameters

• Common name: Reduced Tetradecamolybdate
• Formula: C52 H115 Mo14 N2 O52.5
• Calculated formula: C48 H100 Mo14 N2 O51
• Title of publication: Isolation of stable lacunary Dawson-type structure in a polyoxomolybdate cluster
• Authors of publication: Akihiko Hashikawa; Makkiko Fujimoto; Yoshihito Hayashi; Hitoshi Miyasaka
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 12361
• a: 27.566 ± 0.004 Å
• b: 14.6753 ± 0.0019 Å
• c: 25.184 ± 0.004 Å
• α: 90°
• β: 106.695 ± 0.003°
• γ: 90°
• Cell volume: 9758 ± 2 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0847
• Residual factor for significantly intense reflections: 0.0702
• Weighted residual factors for significantly intense reflections: 0.1314
• Weighted residual factors for all reflections included in the refinement: 0.1387
• Goodness-of-fit parameter for all reflections included in the refinement: 1.225
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No