Information card for entry 7107063

Structure parameters

• Formula: C31 H36 Al4 Cl11 P2 Sb
• Calculated formula: C25 H22 Al2 Cl9 P2 Sb
• SMILES: [Sb]1(Cl)[P](C[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1.[Cl-][Al](Cl)(Cl)Cl.[Cl-][Al](Cl)(Cl)Cl
• Title of publication: Structural diversity for phosphine complexes of stibenium and stibinidenium cations
• Authors of publication: Saurabh S. Chitnis; Brendan Peters; Eamonn Conrad; Neil Burford; Robert McDonald; Michael J. Ferguson
• Journal of publication: Chem.Commun.
• Year of publication: 2011
• Journal volume: 47
• Pages of publication: 12331
• a: 16.299 ± 0.002 Å
• b: 10.3844 ± 0.0015 Å
• c: 25.251 ± 0.004 Å
• α: 90°
• β: 98.272 ± 0.002°
• γ: 90°
• Cell volume: 4229.4 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0576
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for significantly intense reflections: 0.1216
• Weighted residual factors for all reflections included in the refinement: 0.1257
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No