Information card for entry 7107120

Structure parameters

• Formula: C76 H66 Au O7.5 P2 Si2
• Calculated formula: C76 H66 Au O7.5 P2 Si2
• Title of publication: Phosphate ligands in the gold(I)-catalysed activation of enynes
• Authors of publication: Mihai Raducan; Maria Moreno; Christophe Bour; Antonio M. Echavarren
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 52
• a: 11.7382 ± 0.0012 Å
• b: 14.4403 ± 0.0014 Å
• c: 40.493 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6863.7 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0644
• Residual factor for significantly intense reflections: 0.0588
• Weighted residual factors for significantly intense reflections: 0.1424
• Weighted residual factors for all reflections included in the refinement: 0.1464
• Goodness-of-fit parameter for all reflections included in the refinement: 1.142
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No