Information card for entry 7107128

Structure parameters

• Formula: C159.5 H278 Cl36 O P16 Pd8
• Calculated formula: C159.48 H277.8 Cl36 O1.2 P16 Pd8
• Title of publication: A 2,2',6,6'-tetraphosphinobiphenyl
• Authors of publication: Holm Petzold; Albara I. S. Alrawashdeh
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 160
• a: 23.3722 ± 0.0004 Å
• b: 11.654 ± 0.0002 Å
• c: 38.7341 ± 0.0006 Å
• α: 90°
• β: 99.158 ± 0.002°
• γ: 90°
• Cell volume: 10415.9 ± 0.3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0527
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.1027
• Weighted residual factors for all reflections included in the refinement: 0.1058
• Goodness-of-fit parameter for all reflections included in the refinement: 1.072
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No