Crystallography Open Database

Information card for entry 7107254

Preview

Coordinates	7107254.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	4
Formula	C61 H78 Cl12 N4 O4 Rh2 Si2
Calculated formula	C61 H78 Cl12 N4 O4 Rh2 Si2
Title of publication	Efficient generation of stable adducts of Si(II) dihydride
Authors of publication	SM Ibrahim Al-Rafia; Adam C. Malcolm; Robert McDonald; Michael J. Ferguson; Eric Rivard
Journal of publication	Chem.Commun.
Year of publication	2012
Journal volume	48
Pages of publication	1308
a	13.2122 ± 0.0002 Å
b	21.241 ± 0.0003 Å
c	13.2241 ± 0.0002 Å
α	90°
β	97.4269 ± 0.0006°
γ	90°
Cell volume	3680.08 ± 0.09 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0476
Residual factor for significantly intense reflections	0.0452
Weighted residual factors for significantly intense reflections	0.1291
Weighted residual factors for all reflections included in the refinement	0.1316
Goodness-of-fit parameter for all reflections included in the refinement	1.077
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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