Information card for entry 7107384

Structure parameters

• Formula: C24 H30 N4
• Calculated formula: C24 H30 N4
• Title of publication: Iodine-mediated regioselective C2-amination of indoles and a concise total synthesis of (+/-)-folicanthine
• Authors of publication: Ying-Xiu Li; Hai-Xi Wang; Shaukat Ali; Xiao-Feng Xia; Yong-Ming Liang
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 2343
• a: 28.442 ± 0.008 Å
• b: 16.06 ± 0.005 Å
• c: 13.506 ± 0.004 Å
• α: 90°
• β: 90.289 ± 0.003°
• γ: 90°
• Cell volume: 6169 ± 3 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 3
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1176
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for significantly intense reflections: 0.1116
• Weighted residual factors for all reflections included in the refinement: 0.1406
• Goodness-of-fit parameter for all reflections included in the refinement: 1.006
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No