Information card for entry 7107495

Structure parameters

• Formula: C44 H70 Cl Ir N5 Sc
• Calculated formula: C44 H70 Cl Ir N5 Sc
• Title of publication: Reactivity of scandium terminal imido complexes towards metal halides
• Authors of publication: Erli Lu; Qinghai Zhou; Yuxue Li; Jiaxiang Chu; Yaofeng Chen; Xuebing Leng; Jie Sun
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 3403
• a: 23.527 ± 0.003 Å
• b: 12.3238 ± 0.0013 Å
• c: 15.6154 ± 0.0016 Å
• α: 90°
• β: 105.94 ± 0.002°
• γ: 90°
• Cell volume: 4353.5 ± 0.8 ų
• Cell temperature: 133 ± 2 K
• Ambient diffraction temperature: 133 ± 2 K
• Number of distinct elements: 6
• Space group number: 9
• Hermann-Mauguin space group symbol: C 1 c 1
• Hall space group symbol: C -2yc
• Residual factor for all reflections: 0.0311
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for significantly intense reflections: 0.0626
• Weighted residual factors for all reflections included in the refinement: 0.0645
• Goodness-of-fit parameter for all reflections included in the refinement: 1.01
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No