Crystallography Open Database

Information card for entry 7107522

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Coordinates	7107522.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C63 H94 Cl2 Ge N2 P2
Calculated formula	C63 H94 Cl2 Ge N2 P2
Title of publication	Phosphaalkenyl germylenes and their gold, tungsten and molybdenum complexes
Authors of publication	Dimitri Matioszek; Tibor Kocsor; Annie Castel; Gabriela Nemes; Jean Escudie; Nathalie Saffon
Journal of publication	Chem.Commun.
Year of publication	2012
Journal volume	48
Pages of publication	3629
a	13.9844 ± 0.0004 Å
b	14.083 ± 0.0004 Å
c	18.5657 ± 0.0006 Å
α	79.519 ± 0.001°
β	75.857 ± 0.001°
γ	63.285 ± 0.001°
Cell volume	3156.09 ± 0.17 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.073
Residual factor for significantly intense reflections	0.0458
Weighted residual factors for significantly intense reflections	0.1114
Weighted residual factors for all reflections included in the refinement	0.1262
Goodness-of-fit parameter for all reflections included in the refinement	1.019
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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