Crystallography Open Database

Information card for entry 7107549

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Coordinates	7107549.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C51 H75 O8 Pb Sn
Calculated formula	C51 H75 O8 Pb Sn
Title of publication	Stannylplumbylenes: bonding between tetravalent tin and divalent lead
Authors of publication	Drost, Christian; Lönnecke, Peter; Sieler, Joachim
Journal of publication	Chemical Communications (Cambridge, United Kingdom)
Year of publication	2012
Journal volume	48
Journal issue	31
Pages of publication	3778 - 3780
a	26.98 ± 0.0017 Å
b	12.5178 ± 0.0006 Å
c	31.719 ± 0.002 Å
α	90°
β	97.596 ± 0.008°
γ	90°
Cell volume	10618.5 ± 1.1 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0575
Residual factor for significantly intense reflections	0.0296
Weighted residual factors for significantly intense reflections	0.0574
Weighted residual factors for all reflections included in the refinement	0.0608
Goodness-of-fit parameter for all reflections included in the refinement	0.733
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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