Information card for entry 7107775

Structure parameters

• Formula: C21.5 H31 Cl2 F N O3.5 Pt S
• Calculated formula: C21.5 H31 Cl2 F N O3.5 Pt S
• Title of publication: Concerted reductive coupling of an alkyl chloride at Pt(IV)
• Authors of publication: Sarah H. Crosby; Helen R. Thomas; Guy J. Clarkson; Jonathan P. Rourke
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 5775
• a: 9.8916 ± 0.0004 Å
• b: 10.339 ± 0.0005 Å
• c: 13.0249 ± 0.0004 Å
• α: 103.566 ± 0.004°
• β: 95.759 ± 0.003°
• γ: 105.831 ± 0.004°
• Cell volume: 1226.39 ± 0.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0353
• Residual factor for significantly intense reflections: 0.0302
• Weighted residual factors for significantly intense reflections: 0.0751
• Weighted residual factors for all reflections included in the refinement: 0.0762
• Goodness-of-fit parameter for all reflections included in the refinement: 1.102
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No