Information card for entry 7107858

Structure parameters

• Formula: C34 H36 Cu4 N10 O11
• Calculated formula: C34 H36 Cu4 N10 O11
• Title of publication: Copper-induced N-N bond cleavage results in an octanuclear expanded-core grid-like complex
• Authors of publication: Nicholas G. White; Jonathan A. Kitchen; John A. Joule; Sally Brooker
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 6229
• a: 14.973 ± 0.003 Å
• b: 12.682 ± 0.002 Å
• c: 20.506 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3893.8 ± 1.1 ų
• Cell temperature: 91 ± 2 K
• Ambient diffraction temperature: 91 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.1108
• Residual factor for significantly intense reflections: 0.0676
• Weighted residual factors for significantly intense reflections: 0.1431
• Weighted residual factors for all reflections included in the refinement: 0.1674
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No