Crystallography Open Database

Information card for entry 7107914

Preview

Coordinates	7107914.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H46 B9 P2 Rh
Calculated formula	C36 H46 B9 P2 Rh
Title of publication	Zwitterionic half-sandwich Rh and Ir complexes containing a diphosphine nido-carborane ligand: synthesis, structure transformation and application in H2 activation
Authors of publication	Zi-Jian Yao; Xian-Kuan Huo; Guo-Xin Jin
Journal of publication	Chem.Commun.
Year of publication	2012
Journal volume	48
Pages of publication	6714
a	9.646 ± 0.003 Å
b	19.419 ± 0.006 Å
c	10.436 ± 0.003 Å
α	90°
β	110.175 ± 0.003°
γ	90°
Cell volume	1834.9 ± 1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0588
Residual factor for significantly intense reflections	0.0488
Weighted residual factors for significantly intense reflections	0.1288
Weighted residual factors for all reflections included in the refinement	0.1358
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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