Information card for entry 7107941

Structure parameters

• Formula: C14 H16 O17 P2 V3
• Calculated formula: C14 H16 O17 P2 V3
• Title of publication: An enantioenriched vanadium phosphonate generated via asymmetric chiral amplification of crystallization from achiral sources showing a single-crystal-to-single-crystal dehydration process
• Authors of publication: Xiao-Jing Yang; Song-Song Bao; Tao Zheng; Li-Min Zheng
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 6565
• a: 14.478 ± 0.004 Å
• b: 9.033 ± 0.002 Å
• c: 9.404 ± 0.002 Å
• α: 90°
• β: 96.109 ± 0.006°
• γ: 90°
• Cell volume: 1222.9 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1073
• Residual factor for significantly intense reflections: 0.064
• Weighted residual factors for significantly intense reflections: 0.1531
• Weighted residual factors for all reflections included in the refinement: 0.172
• Goodness-of-fit parameter for all reflections included in the refinement: 0.992
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No