Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 7107979
Preview
Coordinates | 7107979.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | Ni(N(SiMe3)(DIPP))2 |
---|---|
Formula | C30 H52 N2 Ni Si2 |
Calculated formula | C30 H52 N2 Ni Si2 |
SMILES | c1(c(cccc1C(C)C)C(C)C)N([Ni]N(c1c(cccc1C(C)C)C(C)C)[Si](C)(C)C)[Si](C)(C)C |
Title of publication | Synthesis and reactivity of a conveniently prepared two-coordinate bis(amido) nickel(II) complex |
Authors of publication | Michael Lipschutz; T.Don Tilley |
Journal of publication | Chem.Commun. |
Year of publication | 2012 |
Journal volume | 48 |
Pages of publication | 7146 |
a | 8.9248 ± 0.0004 Å |
b | 9.168 ± 0.0004 Å |
c | 10.9493 ± 0.0005 Å |
α | 102.092 ± 0.002° |
β | 92.571 ± 0.002° |
γ | 114.391 ± 0.002° |
Cell volume | 789.11 ± 0.06 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.026 |
Residual factor for significantly intense reflections | 0.0241 |
Weighted residual factors for significantly intense reflections | 0.0645 |
Weighted residual factors for all reflections included in the refinement | 0.0658 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.061 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7107979.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.