Information card for entry 7107983

Structure parameters

• Common name: diazo-bis-DIPP
• Formula: C24 H34 N2
• Calculated formula: C24 H34 N2
• SMILES: c1(c(cccc1C(C)C)C(C)C)/N=N/c1c(cccc1C(C)C)C(C)C
• Title of publication: Synthesis and reactivity of a conveniently prepared two-coordinate bis(amido) nickel(II) complex
• Authors of publication: Michael Lipschutz; T.Don Tilley
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 7146
• a: 16.2978 ± 0.0009 Å
• b: 9.4465 ± 0.0005 Å
• c: 13.756 ± 0.0008 Å
• α: 90°
• β: 100.003 ± 0.002°
• γ: 90°
• Cell volume: 2085.6 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0553
• Residual factor for significantly intense reflections: 0.0392
• Weighted residual factors for significantly intense reflections: 0.0901
• Weighted residual factors for all reflections included in the refinement: 0.0991
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No