Information card for entry 7108012

Structure parameters

• Formula: C5 H15 Cl P2
• Calculated formula: C5 H15 Cl P2
• Title of publication: P-P Menschutkin preparation of prototypical phosphinophosphonium salts
• Authors of publication: Saurabh S. Chitnis; Elizabeth MacDonald; Neil Burford; Ulrike Werner-Zwanziger; Robert McDonald
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 7359
• a: 9.4581 ± 0.0006 Å
• b: 6.5601 ± 0.0004 Å
• c: 7.306 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 453.31 ± 0.05 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 31
• Hermann-Mauguin space group symbol: P m n 21
• Hall space group symbol: P 2ac -2
• Residual factor for all reflections: 0.0183
• Residual factor for significantly intense reflections: 0.0177
• Weighted residual factors for significantly intense reflections: 0.0461
• Weighted residual factors for all reflections included in the refinement: 0.0465
• Goodness-of-fit parameter for all reflections included in the refinement: 1.11
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No