Information card for entry 7108162

Structure parameters

• Formula: C18 H22 O8 Pd4
• Calculated formula: C18 H22 O8 Pd4
• SMILES: C1(C)=[O][Pd]23[O]=C(C)O[Pd]456([CH]7=[CH]8[CH]9=[CH]%10[CH]74[Pd]6%10([O]=C(C)O2)([O]=C(C)O3)[Pd]2345689[cH]5[cH]2[cH]3[cH]4[cH]56)O1
• Title of publication: Stabilisation of a triply-bridging cyclopentadienyl ligand in a tetrapalladium cluster
• Authors of publication: Kirill Monakhov; Christophe Gourlaouen; Pierre Braunstein
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 8317
• a: 30.142 ± 0.004 Å
• b: 8.6063 ± 0.001 Å
• c: 18.248 ± 0.002 Å
• α: 90°
• β: 90.703 ± 0.003°
• γ: 90°
• Cell volume: 4733.4 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1125
• Residual factor for significantly intense reflections: 0.0674
• Weighted residual factors for significantly intense reflections: 0.1518
• Weighted residual factors for all reflections included in the refinement: 0.1693
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No