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Information card for entry 7108174
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Coordinates | 7108174.cif |
---|---|
Original paper (by DOI) | HTML |
Chemical name | tetradecalithium-tetrakis[2,6-dimesitylphenyl-disulfido-silanolate] dichloride-5-benzene |
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Formula | C126 H130 Cl2 Li14 O4 S8 Si4 |
Calculated formula | C126 H130 Cl2 Li14 O4 S8 Si4 |
Title of publication | A 32 vertex polyhedron via supramolecular assembly of silanedithiolate silanolate units |
Authors of publication | Stefan Spirk; Ferdinand Belaj; Natascha Hurkes; Rudolf Pietschnig |
Journal of publication | Chem.Commun. |
Year of publication | 2012 |
Journal volume | 48 |
Pages of publication | 8398 |
a | 14.445 ± 0.002 Å |
b | 16.804 ± 0.003 Å |
c | 27.691 ± 0.003 Å |
α | 102.661 ± 0.013° |
β | 90.088 ± 0.012° |
γ | 110.203 ± 0.013° |
Cell volume | 6132.7 ± 1.7 Å3 |
Cell temperature | 95 ± 2 K |
Ambient diffraction temperature | 95 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0655 |
Residual factor for significantly intense reflections | 0.0476 |
Weighted residual factors for significantly intense reflections | 0.1098 |
Weighted residual factors for all reflections included in the refinement | 0.1209 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
Diffraction radiation wavelength | 0.71069 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/7108174.html
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