Information card for entry 7108202

Structure parameters

• Formula: C0 H33 Ge3.3 K6 N11 O0 Si4.7 Zn
• Calculated formula: Ge3.297 H33 K6 N11 Si4.703 Zn
• Title of publication: [(eta^2^-(Si/Ge)4)Zn(eta^2^-(Si/Ge)4)]^6-^ ‒ novel Zintl clusters with mixed Si/Ge tetrahedra bridged by a Zn atom
• Authors of publication: Markus Waibel; Thomas Henneberger; Thomas F. Faessler
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 8676
• a: 9.0694 ± 0.0005 Å
• b: 11.4274 ± 0.0005 Å
• c: 15.8894 ± 0.0008 Å
• α: 77.468 ± 0.004°
• β: 81.547 ± 0.004°
• γ: 87.07 ± 0.004°
• Cell volume: 1589.76 ± 0.14 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0895
• Residual factor for significantly intense reflections: 0.0413
• Weighted residual factors for significantly intense reflections: 0.0785
• Weighted residual factors for all reflections included in the refinement: 0.0863
• Goodness-of-fit parameter for all reflections included in the refinement: 0.79
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No