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Information card for entry 7108359
Preview
Coordinates | 7108359.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C25 H29 Cl F6 N3 O P |
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Calculated formula | C25 H29 Cl F6 N3 O P |
SMILES | c1cc(cc2c1C(=c1ccc(cc1O2)=[N+]1CCCCC1)Cl)N1CCCCC1.[P](F)(F)(F)(F)(F)[F-].CC#N |
Title of publication | Synthesis of new cyclic aromatic carbene ligands bearing remote amino groups and their palladium(II) complexes |
Authors of publication | Shun Sugawara; Satoshi Kojima; Yohsuke Yamamoto |
Journal of publication | Chem.Commun. |
Year of publication | 2012 |
Journal volume | 48 |
Pages of publication | 9735 |
a | 9.0244 ± 0.001 Å |
b | 11.0496 ± 0.0012 Å |
c | 14.0165 ± 0.0015 Å |
α | 103.63 ± 0.003° |
β | 91.184 ± 0.003° |
γ | 109.38 ± 0.003° |
Cell volume | 1273.9 ± 0.2 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0634 |
Residual factor for significantly intense reflections | 0.0511 |
Weighted residual factors for significantly intense reflections | 0.1411 |
Weighted residual factors for all reflections included in the refinement | 0.1503 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.068 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7108359.html
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Users of the data should acknowledge the original authors of the
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