Crystallography Open Database

Information card for entry 7108395

Preview

Coordinates	7108395.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H84 Ge2 N4
Calculated formula	C66 H84 Ge2 N4
Title of publication	An N-heterocyclic carbene adduct of diatomic tin, :Sn[double bond, length as m-dash]Sn:
Authors of publication	Cameron Jones; Anastas Sidiropoulos; Nicole Holzmann; Gernot Frenking; Andreas Stasch
Journal of publication	Chem.Commun.
Year of publication	2012
Journal volume	48
Pages of publication	9855
a	12.2068 ± 0.0002 Å
b	13.3207 ± 0.0003 Å
c	20.7196 ± 0.0004 Å
α	92.467 ± 0.001°
β	93.122 ± 0.001°
γ	116.634 ± 0.001°
Cell volume	2998.5 ± 0.11 Å³
Cell temperature	123 ± 2 K
Ambient diffraction temperature	123 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0658
Residual factor for significantly intense reflections	0.0381
Weighted residual factors for significantly intense reflections	0.0772
Weighted residual factors for all reflections included in the refinement	0.0859
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7108395.html