Information card for entry 7108485

Structure parameters

• Common name: bis((1,4,7,10,13,16-hexaoxacyclooctadecane)-potassium) di- bismuth-di-tin ammoniate
• Chemical name: bis((1,4,7,10,13,16-hexaoxacyclooctadecane)-potassium) di-bismuth-di-tin ammoniate
• Formula: C24 H54 Bi2 K2 N2 O12 Sn2
• Calculated formula: C24 H51 Bi2 K2 N2 O12 Sn2
• Title of publication: Synthesis of Heteroatomic Zintl Anions in Liquid Ammonia - the New Highly Charged [Sn~4~Bi~4~]^ 4‒^ and Fully Ordered [Sn~2~Bi~2~] ^2‒^
• Authors of publication: Ute Friedrich; Maria Neumeier; Carina Koch; Nikolaus Korber
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 10544
• a: 10.4079 ± 0.0007 Å
• b: 14.4988 ± 0.001 Å
• c: 27.679 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4176.8 ± 0.5 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0445
• Residual factor for significantly intense reflections: 0.0352
• Weighted residual factors for significantly intense reflections: 0.0854
• Weighted residual factors for all reflections included in the refinement: 0.0887
• Goodness-of-fit parameter for all reflections included in the refinement: 0.944
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No