Information card for entry 7108637

Structure parameters

• Formula: C30 H10 B F20 N P
• Calculated formula: C30 H10 B F20 N P
• Title of publication: Anomalous Staudinger reaction at intramolecular frustrated P-B Lewis pair frameworks
• Authors of publication: Annika Stute; Lukas Heletta; Roland Frohlich; Constantin G. Daniliuc; Gerald Kehr; Gerhard Erker
• Journal of publication: Chem.Commun.
• Year of publication: 2012
• Journal volume: 48
• Pages of publication: 11739
• a: 10.1955 ± 0.0005 Å
• b: 11.4489 ± 0.0005 Å
• c: 14.1284 ± 0.0005 Å
• α: 66.764 ± 0.002°
• β: 78.902 ± 0.003°
• γ: 89.099 ± 0.003°
• Cell volume: 1483.74 ± 0.11 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0781
• Residual factor for significantly intense reflections: 0.0584
• Weighted residual factors for significantly intense reflections: 0.1457
• Weighted residual factors for all reflections included in the refinement: 0.1646
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No