Information card for entry 7108654

Structure parameters

• Formula: C59 H81 N6 O2 Yb
• Calculated formula: C59 H81 N6 O2 Yb
• Title of publication: Rare-earth metal complexes having an unusual indolyl-1,2-dianion through C‒H activation with a novel η1:(μ2‒η1:η1) bonding with metals
• Authors of publication: Zhu, Xiancui; Zhou, Shuangliu; Wang, Shaowu; Wei, Yun; Zhang, Lijun; Wang, Fenhua; Wang, Shaoyin; Feng, Zhijun
• Journal of publication: Chemical Communications (Cambridge, United Kingdom)
• Year of publication: 2012
• Journal volume: 48
• Journal issue: 98
• Pages of publication: 12020 - 12022
• a: 11.9972 ± 0.0008 Å
• b: 13.3074 ± 0.0009 Å
• c: 21.3606 ± 0.0015 Å
• α: 105.787 ± 0.001°
• β: 102.553 ± 0.001°
• γ: 92.619 ± 0.001°
• Cell volume: 3183.2 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.041
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.0855
• Weighted residual factors for all reflections included in the refinement: 0.0892
• Goodness-of-fit parameter for all reflections included in the refinement: 0.983
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No